The best news is: IT WORKS! The slapback echo is gone and the room doesn't feel dead.

I was sort of hoping that would be the case!
It actually worked rather too well, probably because the absorbers are thicker.
I expected that: That's why I mentioned adding the random slats in the other post. You might need that, but wait and see...
The RT60 time is around 165ms now, my target zone is around 180-200.
165 is a little low, yes, but not shabby at all for that room. It could come up a bit, especially in the low-mids, but I wouldn't be too concerned about it. More important than hitting a specific overall time, is getting the times consistent between adjacent frequency bands... and you are certainly doing that! (see graphs below)...
That could be brought back with some slats, but probably better after the flooring and desk is in place (and the fabrics all around the room)?
Right. Fabric will take the edge of the highs as well.
I wasn't expecting it, but the sound changed quite dramatically - it's like the fog has lifted.

Yup! Diffusers will do that for ya, and polys are especially nice for doing that. Side wall treatment in general is very helpful here.
I thought the speakers were revealing before, but now - this is revealing. The backing vocals suddenly became separate singers, where I heard one distorted guitar I now can hear several different guitars playing at once.

"I love it when a plan comes together!". That's the major goal for a control room: clarity, clear stereo image, and accurate, precise sound stage. You got it! Well done! Even some so-called "pro" rooms sometimes can't achieve that convincingly.
Interestingly even the bass frequencies are a little bit smoother.
Right! Because you are treating your width axials for the first time. Before this, there was nothing to deal with the modes running across the room (as well as the flutter), but now there is.
Many thanks Stuart - your design works, as always

Thanks for the kind words, Martin! I'm pleased that you are seeing (and hearing!) good results, after all the work you put into this place. It's all paying off, now.
OK, so let's take a look at what you accomplished with those polys and absorbers, with some more detailed REW analysis. Here's a series of "before and after" graphs, showing various aspects....
First up, and perhaps the most impressive, is full-spectrum, unsmoothed waterfalls.
BEFORE:
Martin-K--REW--WF-20-20k--Ceiling-done.jpg
AFTER:
Martin-K--REW--WF-20-20k--Side-polys.jpg
You can clearly, clearly see just how bad it was, with all that nasty ringing going on at specific frequencies. There were around 20 very large, very long spikes there before, and all of that has gone now. The difference is day-and-night. That's where all your clarity is coming from. That's why the "fog has lifted". All of that "mush" is wiped out, so now you can hear the pure, clean, direct sound.
Next up: Spectrograms of only the low end.
BEFORE:
Martin-K--REW--SP-18-500--Ceiling-done.jpg
AFTER:
Martin-K--REW--SP-18-500--Side-polys.jpg
Maybe not so dramatic as the waterfalls, but you can still clearly see what you accomplished, and why the bass sounds smoother now. The low end is coming along very nicely!
Now for decay times (RT-60):
BEFORE:
Martin-K--REW--RT--50-10k--Ceiling-done.jpg
AFTER:
Martin-K--REW--RT--50-10k--Side-polys.jpg
Now you can see what I'm talking about regarding decay times consistency between frequency bands. Before, it was all over the place! Each frequency band had a different decay time, with large differences. Eg: look at the difference between 400 Hz and 500 Hz "before": 400 Hz was over 430ms decay, while the very next band up was 240ms, and the very next band down was 215ms. Those are MAJOR swings, well over 200 ms. And AFTER, they are all practically identical: 400 Hz is 135 ms, the next band up is 160ms, and the next band down is 145 ms. Differences of just 15 to 25 milliseconds! Specifications say that it should be no more than 50ms difference between adjacent bands and you are already twice as good as that!

This is more important than hitting a perfect target time: smoothness beats pure numbers here.
And finally, one that isn't commonly even checked by many people, but is really important: Phase response:
BEFORE:
Martin-K--REW--FR.PH--18-2k--Ceiling-done.jpg
AFTER:
Martin-K--REW--FR.PH--18-2k--Side-polys.jpg
It's not so much the actual phase that we are interested in here, but rather how the phase CHANGES over the spectrum, compared to the ideal phase response. That's what the "excess phase" graphs shows (it's more complex than that, but a simple explanation suffices here). As you can see, before the polys, you had major, huge jumps in phase response, but now the phase response is smooth and clean: phase is rotating exactly as it should.
So, yeah, I think it's safe to say that those devices are doing what I designed them to do! And the REW data is just confirming what your ears are already telling you: that's a really nice, clean, smooth, accurate, room now! Congratulations!
- Stuart -