Hi James, and welcome to the forum!
its small 4.3 x 2.3 x 2.8 Meters
So the height is 2.8m, and the width is only 2.3 m? That's unusual, but at least you have good height. You should try to make the best use of that in your design.
But yes, that's not a good ratio, and part of the reason why it sounds so bad.
I produce EDM so the room will rarely have any live instruments tracked in there so I'm going for a fairly dead sound.
So if this is the tracking room, where's the control room, and how big is it? Tracking rooms and control rooms need different treatment for their different acoustics. And since you don't track live acoustic instruments, there isn't really too much need for fantastic treatment in there: just enough to make it pleasant to work in. Since there won't be any mics recording in there, there's no need to have world-class acoustics (unless you want to, of course!) So this is just basically for tracking things like keyboards, electronic drums, and DI'd bass and electric guitar?
I made a tutorial video about how to make better mixes through knowing your room acoustics
Whoa! But that video is all about MIXING! From what you said above, it seems your room is a tracking room! Now I'm confused...
So this IS control room? As in a single, combined "all-in-one" room, for both tracking and mixing? If so, that's a very different situation. It will need lots of treatment.
I'd love to get any extra input in to that knowledge in the video!
Well, I'd suggest improving the accent of the instructor first! He sounds like an Aussie, or something....

(Sorry! Couldn't resist that! I'm also an Aussie living abroad, so I know what it's like to get comments on your accent all the time...

)
One thing. I did notice from that video is the room sound is pretty bad: It's clear from the sound of your voice (regardless of the accent!) that the room is very reverberant, even in the mid range. So superchunks is not all that you will need.
I'd also suggest that instead of trying to use the DAW to analyze the room, that you show how to use REW to do it. That's what REW is designed for, and it does a fantastic job. In fact, it's the best tool I know of for doing basic acoustic analysis. That will reveal exactly where the issues are with the room. Then you can extrapolate the REW results into the rest of your suggestions. REW is also very accurate, and would help you avoid all the obvious uncertainty that you had in the video in trying to identify frequencies and notes.
I'd also suggest using a more comprehensive room ratio calculator, such as Bob Golds' or Andy Mel's. Those are the best ones I know of. At one point in the video you mention that you aren't sure at what point on the spectrum room modes are close enough together to not be an issue: you suggest 2k, but that's way too high: that's the transition from mids to highs. The answer is more like 200 Hz, the transition from lows to mids. I normally analyze up to 500 Hz, just to be safe, but for most typical home studios, the modal issues are below about 200 Hz. You can clearly see why if you look at Bob Golds' or Andy Mel's calculators, since they both show the modes overlaid on a keyboard, and you can therefore easily see at what point you start having more than one mode per note.
Using roxul AFB with a density of 2.5 pounds per cubic foot
That will work fine.
Cutting in to triangles 24"x24"x ~28" and stacking up as high as the roof will allow ~5'
There's something wrong there! If the sides measure 24" x 24" then the front face will be nearly 34", not 28". 34" superchunks are fine, but 28" is a bit small.
Also, if your ceiling is 2.8m high, then how come you only want to go up to 5' with the superchunks? Why not go all the way? Especially considering that modes terminate in corners, so it is more important to have the trap up in the ceiling-wall-wall tricorner.
Putting giant garbage bags over the traps and wrapping the slack of the bag around itself then bonding the bag with spray on adhesive. This step is to keep the rockwool fibres enclosed and also hold it in place somewhat.
That's not the normal reason for wrapping superchunks in plastic! The usual reason is acoustic: it keeps the highs in the room will allowing the bass through. You only really need to be concerned about fibers for the overhead treatment, on the ceiling: Your cloud will certainly need plastic underneath it, to keep those fibers out of your gear and off you! And superchunks need them to prevent them from sucking out too much of the high end. But other wall treatment does not need it. For example, putting plastic on your first reflection point absorbers on the side walls, would not be useful: in fact, it would defeat the entire purpose of those devices!
I will not be making the bags "airtight" like with a real trap,
The don't need to be airtight! Superchunks are not tuned: they are broadband. There is no resonant cavity in there, and no resonant slots, holes or membranes up front, so there is no need to seal them at all. The purpose of the plastic is not to seal them: it is just to keep them from absorbing too much of the high end, and making the room too dead. So all you really need to do, is to cover the front face of your supercunks with plastic: the sides, top and bottom don't need it.
so I'm going for a fairly dead sound
If it really is a control room, then it cannot be either live or dead: it has to be neutral. That's the entire goal and purpose of a control room: to not affect the sound of the speakers at all! Or rather, as little as possible. A control room should not "color" the sound, either on the frequency domain or the time domain (and therefore also the phase domain). It should be neutral, so that ALL you can hear is the clear, unchanged direct sound of the speakers. The room should be "invisible", acoustically. If it is either "live" or "dead", or if it skews the sound in some other way, then it won't be a good control room, and your mixes won't translate very well.
I just figure its a cheaper option than buying enough tight weave fabric to enclose all of the absorbers.
If you do cover them with fabric, then it should not be tight weave! Fabric for acoustic treatment should NOT affect the sound that passes through it. It should be "breathable" and acoustically transparent. It is only there for aesthetic reasons, not acoustic reasons. It "hides the ugly", keeping the actual guts of the acoustic treatment hidden from the room, while still allowing for the full and free passage of sound through it. Some of the best acoustic fabrics are made by Guilford of Maine, so if you do decide to cover yours, take a look at their catalog first. But in reality, and good quality fabric that is breathable will work just fine.
Then I'll wrap them in the most kitch looking bed sheets I can find from the local thrift store,
Provided that the sheets are mostly natural fiber (eg. cotton) and breathable, then that would work fine very likely, but I'm not so sure about the aesthetics!

Take a look around some local fabric stores: you can probably find some inexpensive open-wave stuff that looks decent, or at least looks much better than a bed sheet!
If they seem unstable I might put in a single screw in the and run some string around the top to stop them falling over
Many forum members have built superchunks in a simple frame with plastic and fabric stretched across the front. The frame can just be basically a rectangular shape, like a picture frame, with the plastic and fabric. It can be attached to the walls or ceiling unobtrusively with a couple of nails or screws. It will hold your superchunk in place quite well, and also look good. Other members have built "superchunks on wheels", with a complete 3D frame all around, so that they can then just wheel the entire thing out to the moving van when they leave. You might want to consider those options.
Thoughts??
Before you do anything at all to your room, I'd suggest running REW on it, exactly as it is right now: empty and sounding really bad. That will tell you exactly what is wrong with the room, and orient you in how to treat it. Superchunks will certainly be needed, no doubt at all about that, but they will just be the beginning. You will also undoubtedly need the rest of the "standard" treatment that all small rooms needed: that goes without saying, too. And REW will also reveal where to put that treatment, and if you need anything more beyond that. If you then do additional REW tests after you install each device, then you'll be able to see the progress by comparing readings: so you'll see what is working at each stage, and what still needs to be treated. It's the only sensible way of treating a room, when you are just starting out learning acoustics. More experienced folks can pretty much decide what needs to be built and where to put it just by looking at the room and listening to it, but even the experienced guys still use things like REW to test and check along the way.
So those would be my suggestions!
- Stuart -